916320-82-6 Di-(4-chlorobenzyl)azodicarboxylate AKSci V9117
 
 
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  V9117    
Di-(4-chlorobenzyl)azodicarboxylate
, 98% (HPLC)
 
DCAD, Bis(4-chlorobenzyl)azodicarboxylate




IDENTITY
CAS Number:916320-82-6
MDL Number:MFCD09265148
MF:C16H12Cl2N2O4
MW:367.19
SPECIFICATIONS & PROPERTIES
Min. Purity Spec:98% (HPLC)
Spectra:NMR, LCMS, FT-IR, HPLC
Physical Form:Orange powder
Melting Point:109-115°C
Long-Term Storage:Store long-term at room temperature
HAZARDOUS MATERIALS INFORMATION
Not hazardous material

REVIEW

 Di-(4-chlorobenzyl)azodicarboxylate (DCAD) is a novel, stable, solid alternative to DEAD and DIAD for a variety of Mitsunobu couplings giving a readily separable hydrazine byproduct that can be recycled.

REFERENCES
[1]Bruce H Lipshutz, David W Chung, Brian Rich, Ricardo Corral, Simplification of the Mitsunobu reaction. Di-p-chlorobenzyl azodicarboxylate: a new azodicarboxylate. Organic letters 2006-10-20
[2] Vivian F Su, Kelly A Jones, Michael Brodsky, Inge The, Quantitative analysis of Hedgehog gradient formation using an inducible expression system. BMC developmental biology 2007-5-9

GHS

Pictograms

Signal Word
Warning

Hazard Statements
H317

Precautionary Statements
P261; P272; P280; P302+P352; P321; P333+P313; P363; P501


Current as of December 1, 2020


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