36982-84-0 2,4,6-Triisopropylbenzenesulfonyl azide, stab. with ca 10% water AKSci A848
 
 
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  A848    
2,4,6-Triisopropylbenzenesulfonyl azide, stab. with ca 10% water
, 98%
 



IDENTITY
CAS Number:36982-84-0
MDL Number:MFCD00859286
MF:C15H23N3O2S
MW:309.43
SPECIFICATIONS & PROPERTIES
Min. Purity Spec:98%
Physical Form:White to off-white to yellow powder, solid or crystalline powder
Melting Point:38-46°C
Flash Point:110°C
Long-Term Storage:Store long-term at 2-8°C
HAZARDOUS MATERIALS INFORMATION
Not hazardous material

REVIEW

 Reagent for diazo transfer to ketones, e.g. under phase-transfer conditions, giving better yields of sterically-hindered α-diazo ketones than other methods.

REFERENCES
[1]Synthesis, 368 (1980)
[2] Tetrahedron, 43, 5677 (1987)
[3] J. Am. Chem. Soc., 102, 6626 (1980); 113, 2598 (1991)

GHS

Pictograms

Signal Word
Danger

Hazard Statements
H241; H315; H319; H335; H301+H331

Precautionary Statements
P270; P261; P271; P280; P234; P235; P235+P410; P403+P235; P411+P235; P302+P352; P332+P313; P362; P305+P351+P338; P337+P313; P301+P310+P330; P301+P312+P330; P301+P330+P331; P330; P370+P380; P370+P380+P375; P371+P380+P375; P380; P370+P380+P375; P371+P380+P375; P375; P405; P403+P233; P235+P410; P410; P410+


Current as of September 26, 2020


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CATEGORIES

 Peptide Synthesis > Azides
 Reagents > Azidation
 Reagents > Azidation


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